Adamantane, 1,3-dibromo-
1,3-dibromoadamantane
CAS: 876-53-9
Molecular Formula: C10H14Br2
Adamantane, 1,3-dibromo- - Names and Identifiers
| Name | 1,3-dibromoadamantane |
| Synonyms | NSC 102289 Dibromoadamantane 1,3-Dibromoadamantan 1,3-dibromoadamantane 1,3-DIBROMOADAMANTANE 1,3-DIBROMO- ADAMANTINE Adamantane, 1,3-dibromo- 1,3-dibromotricyclo[3.3.1.1~3,7~]decane 1,3-DIBROMOTRICYCLO[3.3.1.1(3,7)]DECANE tricyclo[3.3.1.1~3,7~]decane, 1,3-dibromo- |
| CAS | 876-53-9 |
| EINECS | 1533716-785-6 |
| InChI | InChI=1/C10H14Br2/c11-9-2-7-1-8(4-9)5-10(12,3-7)6-9/h7-8H,1-6H2 |
| InChIKey | HLWZKLMEOVIWRK-UHFFFAOYSA-N |
Adamantane, 1,3-dibromo- - Physico-chemical Properties
| Molecular Formula | C10H14Br2 |
| Molar Mass | 294.03 |
| Density | 1.864±0.06 g/cm3(Predicted) |
| Melting Point | 108-110 °C (lit.) |
| Boling Point | 287.6±13.0 °C(Predicted) |
| Flash Point | 145.4°C |
| Water Solubility | Soluble in organic solvents,insoluble in water. |
| Solubility | Chloroform (Slightly), Ethyl Acetate (Slightly) |
| Vapor Presure | 0.00425mmHg at 25°C |
| Appearance | Solid |
| Color | White to Pale Gray |
| Storage Condition | Sealed in dry,Room Temperature |
| Refractive Index | 1.651 |
| MDL | MFCD00077218 |
| Use | Is a photosensitive material intermediates, in the pharmaceutical synthesis for a wide range of applications. |
Adamantane, 1,3-dibromo- - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. |
| WGK Germany | 3 |
| Hazard Class | IRRITANT |
Adamantane, 1,3-dibromo- - Reference Information
| Application | is a kind of intermediate of photosensitive material, which has a wide range of applications in pharmaceutical synthesis. |
| production method | add adamantane 13.6g(0.1mol), liquid bromine 40g(0.25mol), iron powder 0.2g. Install reflux condenser and tail gas absorption device, heat reflux reaction at 90 ℃ water bath for 2H, carefully add NaHSO4 solution to soak after the reaction, and recrystallize the crude product with methanol and so on, to obtain product 16.2g,1, the content of 3-dibromoadamantane was 98.3%, the melting point of the product was 110-112 ° C., and the yield was 73.2%. |
Last Update：2024-04-10 22:29:15
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